TY - JOUR
T1 - Electrochemical alternative to obtain reduced graphene oxide by pulse potential: Effect of synthesis parameters and study of corrosion properties
AU - López-Oyama, A. B.
AU - Domínguez-Crespo, M. A.
AU - Torres-Huerta, A. M.
AU - Onofre-Bustamante, E.
AU - Gámez-Corrales, R.
AU - Cayetano-Castro, N.
PY - 2018/9/1
Y1 - 2018/9/1
N2 - © 2018 Two methods to form reduced graphene oxide (rGO) coatings are proposed as simple, rapid and reproducible alternatives to protect 304 L SS substrates. The first route combines traditional Hummers' modified method and pulse electrodeposition technique (−1.6 and −2 VSCE) whereas with the second one, reduction is obtained by applying the potentiostatic method (−1 to −4 VSCE) in a solution containing graphite + H2SO4. The electrochemical results show that ERGO coatings can properly protect metallic substrates only when they are obtained with an applied potential of −4 VSCE. To carry out this process, strong oxidants, extensive water amounts and long reaction times are avoided.
AB - © 2018 Two methods to form reduced graphene oxide (rGO) coatings are proposed as simple, rapid and reproducible alternatives to protect 304 L SS substrates. The first route combines traditional Hummers' modified method and pulse electrodeposition technique (−1.6 and −2 VSCE) whereas with the second one, reduction is obtained by applying the potentiostatic method (−1 to −4 VSCE) in a solution containing graphite + H2SO4. The electrochemical results show that ERGO coatings can properly protect metallic substrates only when they are obtained with an applied potential of −4 VSCE. To carry out this process, strong oxidants, extensive water amounts and long reaction times are avoided.
U2 - 10.1016/j.diamond.2018.04.014
DO - 10.1016/j.diamond.2018.04.014
M3 - Article
SP - 167
EP - 188
JO - Diamond and Related Materials
JF - Diamond and Related Materials
SN - 0925-9635
ER -