Heating rate effects on the TL characteristics of hot filament CVD diamond film

E. Cruz-Zaragoza; S. Gastélum; R. Quispe; R. Meléndrez; M. Pedroza-Montero; M. Barboza-Flores

doi:10.1002/pssa.201000016

Heating rate effects on the TL characteristics of hot filament CVD diamond film

E. Cruz-Zaragoza, S. Gastélum, R. Quispe, R. Meléndrez, M. Pedroza-Montero, M. Barboza-Flores^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

The thermoluminescence (TL) glow curve of polycrystalline chemically vapor deposited (CVD) diamond is strongly dependent on the heating rate used. In the present work, we report results about the heating rate effects on a 500 μm hot filament (HF) CVD diamond film grown on silicon substrate using a precursor gas mixture composition of CH₄(5 sccm)- CO(10 sccm)-H₂(400 sccm). The irradiations were performed with ⁶⁰Co source. The TL measurements were carried out at different heating rates in the 2-30 K/s range. As the heating rate increases, the maximum TL peak intensity decreases and shifts to higher temperature. The shift was from 578 to 669K for heating rates of 2 and 30 K/s, respectively. The kinetics parameter and its dependence on the heating rate were evaluated using the Chen's peak shape method and a computerized glow curve deconvolution (CGCD) method.

Original language	English
Pages (from-to)	2114-2118
Number of pages	5
Journal	Physica Status Solidi (A) Applications and Materials Science
Volume	207
Issue number	9
DOIs	https://doi.org/10.1002/pssa.201000016
State	Published - Sep 2010

Keywords

CVD diamond films
Glow peaks
Heating rate effects
Kinetics parameters
Thermoluminescence

Access to Document

10.1002/pssa.201000016

Cite this

@article{d463e84018a04142a993bcfde4d77623,

title = "Heating rate effects on the TL characteristics of hot filament CVD diamond film",

abstract = "The thermoluminescence (TL) glow curve of polycrystalline chemically vapor deposited (CVD) diamond is strongly dependent on the heating rate used. In the present work, we report results about the heating rate effects on a 500 μm hot filament (HF) CVD diamond film grown on silicon substrate using a precursor gas mixture composition of CH4(5 sccm)- CO(10 sccm)-H2(400 sccm). The irradiations were performed with 60Co source. The TL measurements were carried out at different heating rates in the 2-30 K/s range. As the heating rate increases, the maximum TL peak intensity decreases and shifts to higher temperature. The shift was from 578 to 669K for heating rates of 2 and 30 K/s, respectively. The kinetics parameter and its dependence on the heating rate were evaluated using the Chen's peak shape method and a computerized glow curve deconvolution (CGCD) method.",

keywords = "CVD diamond films, Glow peaks, Heating rate effects, Kinetics parameters, Thermoluminescence",

author = "E. Cruz-Zaragoza and S. Gast{\'e}lum and R. Quispe and R. Mel{\'e}ndrez and M. Pedroza-Montero and M. Barboza-Flores",

year = "2010",

month = sep,

doi = "10.1002/pssa.201000016",

language = "Ingl{\'e}s",

volume = "207",

pages = "2114--2118",

journal = "Physica Status Solidi (A) Applications and Materials Science",

issn = "1862-6300",

publisher = "Wiley-VCH Verlag",

number = "9",

}

TY - JOUR

T1 - Heating rate effects on the TL characteristics of hot filament CVD diamond film

AU - Cruz-Zaragoza, E.

AU - Gastélum, S.

AU - Quispe, R.

AU - Meléndrez, R.

AU - Pedroza-Montero, M.

AU - Barboza-Flores, M.

PY - 2010/9

Y1 - 2010/9

N2 - The thermoluminescence (TL) glow curve of polycrystalline chemically vapor deposited (CVD) diamond is strongly dependent on the heating rate used. In the present work, we report results about the heating rate effects on a 500 μm hot filament (HF) CVD diamond film grown on silicon substrate using a precursor gas mixture composition of CH4(5 sccm)- CO(10 sccm)-H2(400 sccm). The irradiations were performed with 60Co source. The TL measurements were carried out at different heating rates in the 2-30 K/s range. As the heating rate increases, the maximum TL peak intensity decreases and shifts to higher temperature. The shift was from 578 to 669K for heating rates of 2 and 30 K/s, respectively. The kinetics parameter and its dependence on the heating rate were evaluated using the Chen's peak shape method and a computerized glow curve deconvolution (CGCD) method.

AB - The thermoluminescence (TL) glow curve of polycrystalline chemically vapor deposited (CVD) diamond is strongly dependent on the heating rate used. In the present work, we report results about the heating rate effects on a 500 μm hot filament (HF) CVD diamond film grown on silicon substrate using a precursor gas mixture composition of CH4(5 sccm)- CO(10 sccm)-H2(400 sccm). The irradiations were performed with 60Co source. The TL measurements were carried out at different heating rates in the 2-30 K/s range. As the heating rate increases, the maximum TL peak intensity decreases and shifts to higher temperature. The shift was from 578 to 669K for heating rates of 2 and 30 K/s, respectively. The kinetics parameter and its dependence on the heating rate were evaluated using the Chen's peak shape method and a computerized glow curve deconvolution (CGCD) method.

KW - CVD diamond films

KW - Glow peaks

KW - Heating rate effects

KW - Kinetics parameters

KW - Thermoluminescence

UR - http://www.scopus.com/inward/record.url?scp=84922417142&partnerID=8YFLogxK

U2 - 10.1002/pssa.201000016

DO - 10.1002/pssa.201000016

M3 - Artículo

SN - 1862-6300

VL - 207

SP - 2114

EP - 2118

JO - Physica Status Solidi (A) Applications and Materials Science

JF - Physica Status Solidi (A) Applications and Materials Science

IS - 9

ER -

Heating rate effects on the TL characteristics of hot filament CVD diamond film

Abstract

Keywords

Access to Document

Other files and links

Fingerprint

Cite this