TY - JOUR
T1 - Spectroscopic analysis and nuclear magnetic resonance for silver nanoparticles synthesized with trans-resveratrol and cis-resveratrol
AU - Vázquez, Blanca E.Rodríguez
AU - Rodríguez-Beas, Cesar
AU - Iñiguez-Palomares, Ramón Alfonso
AU - Santacruz-Ortega, Hisila
AU - Mendoza-Cruz, Rubén
AU - Bazán-Díaz, Lourdes Soledad
AU - Soberanes, Yedith
AU - Rodríguez-León, Ericka
AU - Navarro, Rosa Elena
N1 - Publisher Copyright:
© 2022, The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.
PY - 2022/5
Y1 - 2022/5
N2 - The synthesis of silver nanoparticles with polyphenolic molecules (AgResvNPs) is important due to potential applications as nanocarriers of resveratrol. Silver nanoparticles were synthesized with trans-3,5,4′-trihydroxystilbene (resveratrol) and irradiated under UV light. Further AgResvNPs were characterized by transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDS), selected area electron diffraction (SAED), UV–Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy with surface-enhanced Raman scattering (SERS), nuclear magnetic resonance (NMR), zeta potential, and dynamic light scattering (DLS) and study of aggregation kinetic and colloidal stability for this system in water and s-DMEM and evaluate the antioxidant capacity with total phenols count assay. Ultraviolet light irradiation promotes the synthesis of AgResvNPs and modifies the conformational structure of resveratrol. NMR confirmed these changes structurally in the molecule. Applications in SERS are an important application of this system.
AB - The synthesis of silver nanoparticles with polyphenolic molecules (AgResvNPs) is important due to potential applications as nanocarriers of resveratrol. Silver nanoparticles were synthesized with trans-3,5,4′-trihydroxystilbene (resveratrol) and irradiated under UV light. Further AgResvNPs were characterized by transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDS), selected area electron diffraction (SAED), UV–Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy with surface-enhanced Raman scattering (SERS), nuclear magnetic resonance (NMR), zeta potential, and dynamic light scattering (DLS) and study of aggregation kinetic and colloidal stability for this system in water and s-DMEM and evaluate the antioxidant capacity with total phenols count assay. Ultraviolet light irradiation promotes the synthesis of AgResvNPs and modifies the conformational structure of resveratrol. NMR confirmed these changes structurally in the molecule. Applications in SERS are an important application of this system.
KW - Electron
KW - Infrared
KW - Microscopy
KW - Nanoparticles
KW - Nuclear magnetic
KW - Optical
KW - Raman scattering
KW - Spectroscopy
UR - http://www.scopus.com/inward/record.url?scp=85124548708&partnerID=8YFLogxK
U2 - 10.1007/s00396-022-04957-3
DO - 10.1007/s00396-022-04957-3
M3 - Artículo
AN - SCOPUS:85124548708
SN - 0303-402X
VL - 300
SP - 465
EP - 475
JO - Colloid and Polymer Science
JF - Colloid and Polymer Science
IS - 5
ER -