Structural and chemical analysis of Zn ion exchange in thermally modified zeolite A4

J. E. Leal-Perez; J. L. Almaral-Sanchez; A. Hurtado-Macias; M. Cortez-Valadez; A. Bórquez-Mendívil; B. A. García-Grajeda; J. M. Mendivil-Escalante; J. Flores-Valenzuela

doi:10.24275/rmiq/Mat24264

Structural and chemical analysis of Zn ion exchange in thermally modified zeolite A4

J. E. Leal-Perez, J. L. Almaral-Sanchez, A. Hurtado-Macias, M. Cortez-Valadez, A. Bórquez-Mendívil, B. A. García-Grajeda, J. M. Mendivil-Escalante, J. Flores-Valenzuela^*

^*Corresponding author for this work

Departamento de Investigación en Física

Research output: Contribution to journal › Article › peer-review

Abstract

This work reports the analysis of Zn ion exchange in thermally modified zeolite A4 (ZA4) for the potential formation of ZnO nanoparticles. The methodology consists of two steps. Step 1 consisted of carrying out different thermal treatments on ZA4. Step 2 involved the ion exchange of Zn with different concentrations of the Zn ion precursor. XRD and FTIR analyses revealed a transformation in the crystal and molecular structure of ZA4 after heat treatment. This work has been limited to studying ion exchange; however, it is very interesting to study the thermal behavior of ZA4 because this could improve the surface area of the material. The results obtained in this work demonstrate that heat treatment and Zn ion concentration affect the crystallinity and molecular structure of ZA4.

Translated title of the contribution	Análisis estructural y químico del intercambio iónico de Zn en zeolita A4 modificada térmicamente
Original language	English
Article number	Mat24264
Journal	Revista Mexicana de Ingeniera Quimica
Volume	23
Issue number	3
DOIs	https://doi.org/10.24275/rmiq/Mat24264
State	Published - 2024

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© 2024, Universidad Autonoma Metropolitana. All rights reserved.

Keywords

Zn
heat treatment
structural analysis
zeolite A4

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10.24275/rmiq/Mat24264

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Leal-Perez, J. E., Almaral-Sanchez, J. L., Hurtado-Macias, A., Cortez-Valadez, M., Bórquez-Mendívil, A., García-Grajeda, B. A., Mendivil-Escalante, J. M., & Flores-Valenzuela, J. (2024). Structural and chemical analysis of Zn ion exchange in thermally modified zeolite A4. Revista Mexicana de Ingeniera Quimica, 23(3), Article Mat24264. https://doi.org/10.24275/rmiq/Mat24264

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abstract = "This work reports the analysis of Zn ion exchange in thermally modified zeolite A4 (ZA4) for the potential formation of ZnO nanoparticles. The methodology consists of two steps. Step 1 consisted of carrying out different thermal treatments on ZA4. Step 2 involved the ion exchange of Zn with different concentrations of the Zn ion precursor. XRD and FTIR analyses revealed a transformation in the crystal and molecular structure of ZA4 after heat treatment. This work has been limited to studying ion exchange; however, it is very interesting to study the thermal behavior of ZA4 because this could improve the surface area of the material. The results obtained in this work demonstrate that heat treatment and Zn ion concentration affect the crystallinity and molecular structure of ZA4.",

keywords = "Zn, heat treatment, structural analysis, zeolite A4",

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doi = "10.24275/rmiq/Mat24264",

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T1 - Structural and chemical analysis of Zn ion exchange in thermally modified zeolite A4

AU - Leal-Perez, J. E.

AU - Almaral-Sanchez, J. L.

AU - Hurtado-Macias, A.

AU - Cortez-Valadez, M.

AU - Bórquez-Mendívil, A.

AU - García-Grajeda, B. A.

AU - Mendivil-Escalante, J. M.

AU - Flores-Valenzuela, J.

PY - 2024

Y1 - 2024

N2 - This work reports the analysis of Zn ion exchange in thermally modified zeolite A4 (ZA4) for the potential formation of ZnO nanoparticles. The methodology consists of two steps. Step 1 consisted of carrying out different thermal treatments on ZA4. Step 2 involved the ion exchange of Zn with different concentrations of the Zn ion precursor. XRD and FTIR analyses revealed a transformation in the crystal and molecular structure of ZA4 after heat treatment. This work has been limited to studying ion exchange; however, it is very interesting to study the thermal behavior of ZA4 because this could improve the surface area of the material. The results obtained in this work demonstrate that heat treatment and Zn ion concentration affect the crystallinity and molecular structure of ZA4.

AB - This work reports the analysis of Zn ion exchange in thermally modified zeolite A4 (ZA4) for the potential formation of ZnO nanoparticles. The methodology consists of two steps. Step 1 consisted of carrying out different thermal treatments on ZA4. Step 2 involved the ion exchange of Zn with different concentrations of the Zn ion precursor. XRD and FTIR analyses revealed a transformation in the crystal and molecular structure of ZA4 after heat treatment. This work has been limited to studying ion exchange; however, it is very interesting to study the thermal behavior of ZA4 because this could improve the surface area of the material. The results obtained in this work demonstrate that heat treatment and Zn ion concentration affect the crystallinity and molecular structure of ZA4.

KW - Zn

KW - heat treatment

KW - structural analysis

KW - zeolite A4

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DO - 10.24275/rmiq/Mat24264

M3 - Artículo

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SN - 1665-2738

VL - 23

JO - Revista Mexicana de Ingeniera Quimica

JF - Revista Mexicana de Ingeniera Quimica

IS - 3

M1 - Mat24264

ER -

Structural and chemical analysis of Zn ion exchange in thermally modified zeolite A4

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