TY - JOUR
T1 - Crystal structure of fully protonated 3,10,20,21,28-tetraoxo-5,8,23,26-tetrakis(carboxymethyl)-2,5,8,11,20,23,26,29-octaaza[12.12]metacyclophane
AU - Altamirano-Coronado, Julio C.
AU - Höpfl, Herbert
AU - Godoy-Alcantar, Carolina
AU - Machi, Lorena
AU - Medrano, Felipe
PY - 2006/1/1
Y1 - 2006/1/1
N2 - A protonated cation salt of title compound C36H48N8O12 crystallized in the monoclinic space group with cell parameters a = 11.4721(8)Å, b = 23.1049(16)Å, c = 21.0730(14)Å, β = 99.0040(10)° and Z = 4; the final residual factor was 0.0582 with 9694 reflections. A cyclophane conformation was determinated by an interplay between the ridigidy of amide and phenyl groups and the presence of intramolecular hydrogen bonds and C-H···π interactions. 2006 © The Japan Society for Analytical Chemistry.
AB - A protonated cation salt of title compound C36H48N8O12 crystallized in the monoclinic space group with cell parameters a = 11.4721(8)Å, b = 23.1049(16)Å, c = 21.0730(14)Å, β = 99.0040(10)° and Z = 4; the final residual factor was 0.0582 with 9694 reflections. A cyclophane conformation was determinated by an interplay between the ridigidy of amide and phenyl groups and the presence of intramolecular hydrogen bonds and C-H···π interactions. 2006 © The Japan Society for Analytical Chemistry.
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U2 - 10.2116/analscix.22.x271
DO - 10.2116/analscix.22.x271
M3 - Note
JO - Analytical Sciences: X-ray Structure Analysis Online
JF - Analytical Sciences: X-ray Structure Analysis Online
SN - 1348-2238
ER -