l-Proline-sodium nitrate obtained from solvent drop grinding

Javier Hernández-Paredes; Francisco Javier Carrillo-Pesqueira; Hilda E. Esparza-Ponce; Ofelia Hernández-Negrete; Mario E. Alvarez-Ramos

doi:10.1016/j.poly.2015.02.034

l-Proline-sodium nitrate obtained from solvent drop grinding

Javier Hernández-Paredes^*, Francisco Javier Carrillo-Pesqueira, Hilda E. Esparza-Ponce, Ofelia Hernández-Negrete, Mario E. Alvarez-Ramos

^*Autor correspondiente de este trabajo

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

4 Citas (Scopus)

Resumen

Abstract l-Proline sodium nitrate was obtained by the solvent drop grinding (SDG) technique. The compound was characterized by X-ray powder diffraction (XRPD), infrared spectroscopy (FTIR) and thermal analysis (DSC/TGA). Additionally, the material was tested for second harmonic generation (SHG). XRPD confirmed the presence of a new phase with a 1:1 stoichiometry and its crystal structure was determined. The FTIR spectroscopy depicted accurately the molecular characteristics of the compound and the thermal analysis showed that the compound is stable below 160 C. Surprisingly, the compound displayed modest NLO properties which were strongly affected by its crystal packing features.

Idioma original	Inglés
Número de artículo	11220
Páginas (desde-hasta)	84-88
Número de páginas	5
Publicación	Polyhedron
Volumen	91
DOI	https://doi.org/10.1016/j.poly.2015.02.034
Estado	Publicada - 8 may. 2015

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© 2015 Elsevier Ltd. All rights reserved.

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@article{aeafc463e9254367b097009752433386,

title = "l-Proline-sodium nitrate obtained from solvent drop grinding",

abstract = "Abstract l-Proline sodium nitrate was obtained by the solvent drop grinding (SDG) technique. The compound was characterized by X-ray powder diffraction (XRPD), infrared spectroscopy (FTIR) and thermal analysis (DSC/TGA). Additionally, the material was tested for second harmonic generation (SHG). XRPD confirmed the presence of a new phase with a 1:1 stoichiometry and its crystal structure was determined. The FTIR spectroscopy depicted accurately the molecular characteristics of the compound and the thermal analysis showed that the compound is stable below 160 C. Surprisingly, the compound displayed modest NLO properties which were strongly affected by its crystal packing features.",

keywords = "Crystal structure, Rietveld refinement, SHG, X-ray diffraction, l-Proline",

author = "Javier Hern{\'a}ndez-Paredes and Carrillo-Pesqueira, {Francisco Javier} and Esparza-Ponce, {Hilda E.} and Ofelia Hern{\'a}ndez-Negrete and Alvarez-Ramos, {Mario E.}",

year = "2015",

month = may,

day = "8",

doi = "10.1016/j.poly.2015.02.034",

language = "Ingl{\'e}s",

volume = "91",

pages = "84--88",

journal = "Polyhedron",

issn = "0277-5387",

publisher = "Elsevier Ltd",

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TY - JOUR

T1 - l-Proline-sodium nitrate obtained from solvent drop grinding

AU - Hernández-Paredes, Javier

AU - Carrillo-Pesqueira, Francisco Javier

AU - Esparza-Ponce, Hilda E.

AU - Hernández-Negrete, Ofelia

AU - Alvarez-Ramos, Mario E.

PY - 2015/5/8

Y1 - 2015/5/8

N2 - Abstract l-Proline sodium nitrate was obtained by the solvent drop grinding (SDG) technique. The compound was characterized by X-ray powder diffraction (XRPD), infrared spectroscopy (FTIR) and thermal analysis (DSC/TGA). Additionally, the material was tested for second harmonic generation (SHG). XRPD confirmed the presence of a new phase with a 1:1 stoichiometry and its crystal structure was determined. The FTIR spectroscopy depicted accurately the molecular characteristics of the compound and the thermal analysis showed that the compound is stable below 160 C. Surprisingly, the compound displayed modest NLO properties which were strongly affected by its crystal packing features.

AB - Abstract l-Proline sodium nitrate was obtained by the solvent drop grinding (SDG) technique. The compound was characterized by X-ray powder diffraction (XRPD), infrared spectroscopy (FTIR) and thermal analysis (DSC/TGA). Additionally, the material was tested for second harmonic generation (SHG). XRPD confirmed the presence of a new phase with a 1:1 stoichiometry and its crystal structure was determined. The FTIR spectroscopy depicted accurately the molecular characteristics of the compound and the thermal analysis showed that the compound is stable below 160 C. Surprisingly, the compound displayed modest NLO properties which were strongly affected by its crystal packing features.

KW - Crystal structure

KW - Rietveld refinement

KW - SHG

KW - X-ray diffraction

KW - l-Proline

UR - http://www.scopus.com/inward/record.url?scp=84925004732&partnerID=8YFLogxK

U2 - 10.1016/j.poly.2015.02.034

DO - 10.1016/j.poly.2015.02.034

M3 - Artículo

SN - 0277-5387

VL - 91

SP - 84

EP - 88

JO - Polyhedron

JF - Polyhedron

M1 - 11220

ER -

l-Proline-sodium nitrate obtained from solvent drop grinding

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